Enhanced electrocatalytic and supercapacitance performances of transition metal oxynitride thin films

Department

College of Mechanical Engineering, North Carolina Agricultural and Technical State University

Document Type

Poster

Publication Date

4-17-2026

Abstract

The importance of research in the field of non-conventional energy generation and storage cannot be overemphasized in order to be less dependent on limited resources in nature. Our research has established the effectiveness of the pulsed laser deposition (PLD) method for the synthesis of an emerging class of transition metal oxynitride (TMON) material systems in epitaxial thin film form. The material systems cover a wide range of compositions that exhibit the physicochemical properties needed in electrocatalysis and extended-life electrochemical energy storage. The attraction of TMONs over more widely studied transition metal oxides (TMOs) is rooted in the polarizability, electronegativity, and anion charge of versus that of oxygen, which induces an enormous change in the physical and chemical properties of the resulting compounds. TMON films were deposited in the presence of oxygen in the PLD chamber. The films were characterized using high resolution x-ray diffraction, x-ray reflectometry techniques, and x-ray photoelectron spectroscopy. The electrochemical supercapacitor measurements on the TiNO films using cyclic voltammetry have shown that the specific capacitance values are amongst the highest values reported for the recently top-tier nanoscale electrode materials.

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